Knowledge Management System of Northwest Institute of Plateau Biology, CAS
Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry | |
Wei, T; Dahua, Z; Cheng, XG; Li, YL; Chen, LR; Li, YM | |
2005-09-01 | |
发表期刊 | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
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卷号 | 33期号:9页码:1265-1268 |
文章类型 | Article |
摘要 | A rapid method was first applied to analyze the extract of the Swertia franchetiana H. Smith with high performance liquid chromatograghy-atmospheric pressure(LC-APCI-MS) and ultraviolet (UV) spectrometry. Five glycosides were well separated on an ODS column (4. 6 mm i.d. x 200 mm, 5 mu m) with mixtures of methanol and water as mobile phase. The recoveries of (1) swertiamarin (2) gentiopicroside (3) sweroside (4) isoorientin and (5) swetianolin fortified in the ranges of 7. 4 similar to 740; 14 similar to 590; 5.2 similar to 525; 4.2 similar to 343; and 1.0 similar to 171 mg/L were 98.3%, 106.7%, 92.3%, 88.2% and 107.3%, respectively. It is suitable for the quality control of the extract from swertia franchetiana H. Smith. |
关键词 | Liquid Chromatography-mass Spectrometry Glycosides Extract Of Swertia FrancH.tiana H. Smith |
WOS标题词 | Science & Technology ; Physical Sciences |
收录类别 | SCI |
语种 | 英语 |
WOS研究方向 | Chemistry |
WOS类目 | Chemistry, Analytical |
WOS记录号 | WOS:000232564600015 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://210.75.249.4/handle/363003/6849 |
专题 | 中国科学院西北高原生物研究所 |
作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China 2.Gansu Inst Drug Control, Lanzhou 730030, Peoples R China 3.PetroChina Co Ltd Lubricant Co, Lanzhou 730060, Peoples R China 4.Chinese Acad Sci, NW Plateau Inst Biol, Xining 810001, Peoples R China |
推荐引用方式 GB/T 7714 | Wei, T,Dahua, Z,Cheng, XG,et al. Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2005,33(9):1265-1268. |
APA | Wei, T,Dahua, Z,Cheng, XG,Li, YL,Chen, LR,&Li, YM.(2005).Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,33(9),1265-1268. |
MLA | Wei, T,et al."Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 33.9(2005):1265-1268. |
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